A microwave-powered continuous fluidic system for polymer nanocomposite manufacturing: A proof-of-concept study

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dc.authorid0000-0002-1677-644X
dc.contributor.authorTorabfam, Milad
dc.contributor.authorNejatpour, Mona
dc.contributor.authorFidan, Tuçe
dc.contributor.authorKurt, Hasan
dc.contributor.authorYüce, Meral
dc.contributor.authorBayazıt, Mustafa Kemal
dc.date.accessioned2022-11-14T09:02:49Z
dc.date.available2022-11-14T09:02:49Z
dc.date.issued2022
dc.departmentİstanbul Medipol Üniversitesi, Mühendislik ve Doğa Bilimleri Fakültesi, Endüstri Mühendisliği Bölümü
dc.departmentİstanbul Medipol Üniversitesi, Rektörlük, Sağlık Bilim ve Teknolojileri Araştırma Enstitüsü
dc.description.abstractContinuous manufacturing of pure nanocrystals with a narrow size distribution in a polymer matrix is very challenging, although it is highly crucial to get their full potential for advanced applications. A long-lasting nanocomposite (NC) manufacturing challenge is, for the first time, overcome by a microwave-powered fluidic system (MWFS). The effect of microwave power (MWP), flow rate, and the concentration of the reagents are systematically studied. The nylon-6 NC bearing evenly distributed silver nanoparticles (AgNPs) with a mean size of similar to 2.59 +/- 0.639 nm is manufactured continuously in similar to 2 min at similar to 50-55 degrees C using a green solvent, formic acid. The AgNP size becomes smaller when increasing the polymer concentration gradually. Small NPs with a narrow size distribution are produced at high MWP (40 W), but large ones with a broad size distribution at low MWP (10 W). The nylon-6 crystallinity is NP size-dependent, and the gamma-phase (pseudo-hexagonal crystal) is dominant in the presence of small NPs as against the large counterparts. Given the small-sized AgNPs in the MWF-manufactured NCs, the antibacterial activity tests with Escherichia coli, Staphylococcus aureus, and Pseudomonas aeruginosa show superior activity compared to that of the large AgNP-bearing (similar to 50 nm) NCs produced in a conventional heating fluidic system. The proposed MWFS can manufacture other added-value NCs continuously.
dc.identifier.citationTorabfam, M., Nejatpour, M., Fidan, T., Kurt, H., Yüce, M. ve Bayazıt, M. K. (2022). A microwave-powered continuous fluidic system for polymer nanocomposite manufacturing: A proof-of-concept study. Green Chemistry, 24(7), 2812-2824. https://doi.org/10.1039/d1gc04711f
dc.identifier.doi10.1039/d1gc04711f
dc.identifier.endpage2824
dc.identifier.issn1463-9262
dc.identifier.issn1463-9270
dc.identifier.issue7
dc.identifier.scopus2-s2.0-85127669630
dc.identifier.scopusqualityQ1
dc.identifier.startpage2812
dc.identifier.urihttps://doi.org/10.1039/d1gc04711f
dc.identifier.urihttps://hdl.handle.net/20.500.12511/9954
dc.identifier.volume24
dc.identifier.wos000770048900001en_US
dc.identifier.wosqualityQ1
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorKurt, Hasan
dc.language.isoen
dc.publisherRoyal Society of Chemistry
dc.relation.ispartofGreen Chemistryen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.relation.tubitakinfo:eu-repo/grantAgreement/TUBITAK/SOBAG/118C316
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectPolymer Nanocomposite Manufacturing
dc.subjectFluidic System
dc.subjectMicrowave
dc.titleA microwave-powered continuous fluidic system for polymer nanocomposite manufacturing: A proof-of-concept study
dc.typeArticle

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