Vacuum carbothermal synthesis of TiB2

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dc.authorid0000-0001-6276-9251
dc.contributor.authorBuğdaycı, Mehmet
dc.contributor.authorGüleç, Şeyma
dc.date.accessioned2023-11-27T10:53:05Z
dc.date.available2023-11-27T10:53:05Z
dc.date.issued2023
dc.departmentİstanbul Medipol Üniversitesi, İMÜ Meslek Yüksekokulu, İnşaat Teknolojisi Ana Bilim Dalı
dc.description.abstractAbstract: In this study, the formation conditions of TiB2, whose main production method is carbothermal reduction, at lower temperatures with additional processes (vacuum, mechanical activation and functional addition effect) were investigated. In this study, firstly the 100% stoichiometric mixture was reduced at 1200°C under vacuum for varying experimental durations. Afterwards, the effect of mechanical activation amount on TiB2 formation was determined by keeping the 4-h reduction time, which was determined as optimum in the first set of experiments. At the last stage of the experiments, the addition of 2.5 and 5% NaCl effect on the mixtures in the first set of experiments was determined. The samples obtained after the experiment were characterized by XRD and SEM techniques, and it was observed that the undesired phases were completely removed as a result of the reduction performed after 16 h of ball mile operation, and this experiment was determined as the optimum experimental condition.
dc.description.sponsorshipYalova Universityen_US
dc.identifier.citationBuğdaycı, M. ve Güleç, Ş. (2023). Vacuum carbothermal synthesis of TiB2. Journal of Superhard Materials, 45(5), 360-369. https://dx.doi.org/10.3103/S1063457623050039
dc.identifier.doi10.3103/S1063457623050039
dc.identifier.endpage369
dc.identifier.issn1063-4576
dc.identifier.issn1934-9408
dc.identifier.issue5
dc.identifier.scopus2-s2.0-85176291999
dc.identifier.scopusqualityQ3
dc.identifier.startpage360
dc.identifier.urihttps://dx.doi.org/10.3103/S1063457623050039
dc.identifier.urihttps://hdl.handle.net/20.500.12511/11880
dc.identifier.volume45
dc.identifier.wos001103678900001en_US
dc.identifier.wosqualityQ4
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.institutionauthorBuğdaycı, Mehmet
dc.language.isoen
dc.publisherPleiades Publishing
dc.relation.ispartofJournal of Superhard Materialsen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/embargoedAccess
dc.subjectBall Mill
dc.subjectCarbothermal Reduction
dc.subjectFact Sage
dc.subjectTiB2
dc.subjectVacuum
dc.titleVacuum carbothermal synthesis of TiB2
dc.typeArticle

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