Combustion synthesis of B4C–TiB2 composite nanoparticle by Self-Propagating High-Temperature Synthesis (SHS) in B2O3–TiO2–Mg–C system

Basit Öğe Kaydı
dc.authorid0000-0002-7933-5887
dc.contributor.authorÇoban, Ozan
dc.contributor.authorBuğdaycı, Mehmet
dc.contributor.authorBaşlayıcı, Serkan
dc.contributor.authorAçma, Mahmut Ercan
dc.date.accessioned2023-04-10T09:00:07Z
dc.date.available2023-04-10T09:00:07Z
dc.date.issued2023
dc.departmentİstanbul Medipol Üniversitesi, İMÜ Meslek Yüksekokulu, İnşaat Teknolojisi Ana Bilim Dalı
dc.description.abstractIn this study, B4C-TiB2 nanocomposite powder was synthesized from oxide raw materials with the principle of magnesiothermic reduction in B2O3–TiO2–Mg–C system by SHS method. For the SHS process, Mg and C stoichiometries were optimized with thermochemical simulation, and composite charge stoichiometry and Mg particle size were optimized with XRD, BET and SEM analyzes. Optimization of acid concentration, leaching temperature, and leaching time parameters has been provided for the HCl leaching processes carried out to remove undesired by-products after SHS. In addition, pH and temperature changes during leaching were analyzed and an innovative application of modified leaching with H2O2 and carbonic acid addition was investigated. The results showed that by optimizing the process steps for the synthesis of B4C–TiB2 composite nanoparticle by the SHS method, a commercial grade product with a surface area of 30.6 m2/g, and a particle size of 193 nm was obtained.
dc.identifier.citationÇoban, O., Buğdaycı, M., Başlayıcı, S. ve Açma, M. E. (2023). Combustion synthesis of B4C–TiB2 composite nanoparticle by Self-Propagating High-Temperature Synthesis (SHS) in B2O3–TiO2–Mg–C system. Advances in Powder and Ceramic Materials Science Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023 içinde (161-169. ss.). San Diego, 19-23 March 2023. https://dx.doi.org/10.1007/978-3-031-22622-9_16
dc.identifier.doi10.1007/978-3-031-22622-9_16
dc.identifier.endpage169
dc.identifier.isbn9783031226212
dc.identifier.issn2367-1181
dc.identifier.scopus2-s2.0-85151136888
dc.identifier.scopusqualityQ3
dc.identifier.startpage161
dc.identifier.urihttps://dx.doi.org/10.1007/978-3-031-22622-9_16
dc.identifier.urihttps://hdl.handle.net/20.500.12511/10839
dc.indekslendigikaynakScopus
dc.institutionauthorBaşlayıcı, Serkan
dc.language.isoen
dc.publisherSpringer Science and Business Media Deutschland GmbH
dc.relation.ispartofAdvances in Powder and Ceramic Materials Science Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023en_US
dc.relation.publicationcategoryKonferans Öğesi - Uluslararası - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectAdvanced Ceramics
dc.subjectBoron Carbide
dc.subjectComposite Powder
dc.subjectNanoparticle Synthesis
dc.subjectTitanium Diboride
dc.titleCombustion synthesis of B4C–TiB2 composite nanoparticle by Self-Propagating High-Temperature Synthesis (SHS) in B2O3–TiO2–Mg–C system
dc.typeConference Object

Dosyalar

Lisans paketi
Listeleniyor 1 - 1 / 1
Küçük Resim Yok
İsim:
license.txt
Boyut:
1.44 KB
Biçim:
Item-specific license agreed upon to submission
Açıklama:
İndir

Koleksiyon

Bildiri Koleksiyonu
Scopus İndeksli Yayınlar Koleksiyonu