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dc.contributor.authorÇoban, Ozan
dc.contributor.authorBuğdaycı, Mehmet
dc.contributor.authorBaşlayıcı, Serkan
dc.contributor.authorAçma, Mahmut Ercan
dc.date.accessioned2023-04-10T09:00:07Z
dc.date.available2023-04-10T09:00:07Z
dc.date.issued2023en_US
dc.identifier.citationÇoban, O., Buğdaycı, M., Başlayıcı, S. ve Açma, M. E. (2023). Combustion synthesis of B4C–TiB2 composite nanoparticle by Self-Propagating High-Temperature Synthesis (SHS) in B2O3–TiO2–Mg–C system. Advances in Powder and Ceramic Materials Science Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023 içinde (161-169. ss.). San Diego, 19-23 March 2023. https://dx.doi.org/10.1007/978-3-031-22622-9_16en_US
dc.identifier.isbn9783031226212
dc.identifier.issn2367-1181
dc.identifier.urihttps://dx.doi.org/10.1007/978-3-031-22622-9_16
dc.identifier.urihttps://hdl.handle.net/20.500.12511/10839
dc.description.abstractIn this study, B4C-TiB2 nanocomposite powder was synthesized from oxide raw materials with the principle of magnesiothermic reduction in B2O3–TiO2–Mg–C system by SHS method. For the SHS process, Mg and C stoichiometries were optimized with thermochemical simulation, and composite charge stoichiometry and Mg particle size were optimized with XRD, BET and SEM analyzes. Optimization of acid concentration, leaching temperature, and leaching time parameters has been provided for the HCl leaching processes carried out to remove undesired by-products after SHS. In addition, pH and temperature changes during leaching were analyzed and an innovative application of modified leaching with H2O2 and carbonic acid addition was investigated. The results showed that by optimizing the process steps for the synthesis of B4C–TiB2 composite nanoparticle by the SHS method, a commercial grade product with a surface area of 30.6 m2/g, and a particle size of 193 nm was obtained.en_US
dc.language.isoengen_US
dc.publisherSpringer Science and Business Media Deutschland GmbHen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectAdvanced Ceramicsen_US
dc.subjectBoron Carbideen_US
dc.subjectComposite Powderen_US
dc.subjectNanoparticle Synthesisen_US
dc.subjectTitanium Diborideen_US
dc.titleCombustion synthesis of B4C–TiB2 composite nanoparticle by Self-Propagating High-Temperature Synthesis (SHS) in B2O3–TiO2–Mg–C systemen_US
dc.typeconferenceObjecten_US
dc.relation.ispartofAdvances in Powder and Ceramic Materials Science Symposium, held at the TMS Annual Meeting and Exhibition, TMS 2023en_US
dc.departmentİstanbul Medipol Üniversitesi, İMÜ Meslek Yüksekokulu, İnşaat Teknolojisi Ana Bilim Dalıen_US
dc.authorid0000-0002-7933-5887en_US
dc.identifier.startpage161en_US
dc.identifier.endpage169en_US
dc.relation.publicationcategoryKonferans Öğesi - Uluslararası - Kurum Öğretim Elemanıen_US
dc.identifier.doi10.1007/978-3-031-22622-9_16en_US
dc.institutionauthorBaşlayıcı, Serkan
dc.identifier.scopus2-s2.0-85151136888en_US
dc.identifier.scopusqualityQ3en_US


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